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Complete characterization of the ceramic-based hot-coated coating on the AZ91 magnesium alloy
Plevová, Kateřina ; Doskočil, Leoš (referee) ; Wasserbauer, Jaromír (advisor)
The diploma thesis is focused on the study of the thermal sprayed coating consisting of the NiCrAlY alloy bond layer and the partially stabilized zirconium oxide (8YSZ) top layer on the AZ91 magnesium alloy. The theoretical part deals with the structure of the alloy AZ91, NiCrAlY and partially stabilized zirconia. Furthermore, the methods of thermal spraying and the function and properties of thermal barrier coatings are summarized. The experimental part deals with the characterization of the thermal sprayed coating and the AZ91 alloy in terms of elemental, structural and phase composition. Optical and electron microscopy, EDS and XRD analysis were used for characterization. Electrochemical properties were investigated in~3.5% sodium chloride solution by potentiodynamic polarization. The mechanical properties (hardness, coefficient of friction) of the substrate and coating were measured using a hardness tester and tribological tests.
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Complete characterization of the ceramic-based hot-coated coating on the AZ91 magnesium alloy
Plevová, Kateřina ; Doskočil, Leoš (referee) ; Wasserbauer, Jaromír (advisor)
The diploma thesis is focused on the study of the thermal sprayed coating consisting of the NiCrAlY alloy bond layer and the partially stabilized zirconium oxide (8YSZ) top layer on the AZ91 magnesium alloy. The theoretical part deals with the structure of the alloy AZ91, NiCrAlY and partially stabilized zirconia. Furthermore, the methods of thermal spraying and the function and properties of thermal barrier coatings are summarized. The experimental part deals with the characterization of the thermal sprayed coating and the AZ91 alloy in terms of elemental, structural and phase composition. Optical and electron microscopy, EDS and XRD analysis were used for characterization. Electrochemical properties were investigated in~3.5% sodium chloride solution by potentiodynamic polarization. The mechanical properties (hardness, coefficient of friction) of the substrate and coating were measured using a hardness tester and tribological tests.
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Měření tvrdosti nehomogenních plazmových nástřiků
Čtvrtlík, Radim ; Stranyánek, Martin ; Boháč, Petr ; Jastrabík, Lubomír ; Hrabovský, Milan ; Ctibor, Pavel
Paper deals with testing of mechanical properties of plasma sprayed coatings TiO2 by Depth Sensing Indentation performed on measuring system NanoTest 600™. The NT600™ is a modular measuring instrument with unique design, which applies the loading force in horizontal direction. The platform can measure and evaluate hardness, elastic modulus, adhesion, wear, fracture and also dynamic properties. In the last years the new plasma spraying technology of ceramic and ceramic-metal materials has became as very convenient technique in many industrial and reconstruction processes. The investigated samples of plasma sprayed coatings were prepared in Institute of Plasma Physics of the Academy of Sciences of the Czech Republic. The goal of this paper is to contribute to deepening the knowledge in local distribution of mechanical properties in plasma sprayed coatings, especially of hardness and elastic modulus.
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